SEM/EDX AND XRD CHARACTERIZATION OF SILVER NANOCRYSTALLINE THIN FILM PREPARED FROM ORGANOMETALLIC SOLUTION PRECURSOR

  • Radovan Ž. Dimitrijević Faculty of Mining and Geology, Department of Crystallography, University of Belgrade, Đušina 7, Belgrade, Serbia
  • Olga G. Cvetković Center of Chemistry, Institute of Chemistry, Technology and Metallurgy (ICTM), University of Belgrade, Njegoševa 12, 11000 Belgrade, Serbia
  • Zoran M. Miodragović Faculty of Chemistry, University of Belgrade, Studentski trg 12-16, 11000 Belgrade, Serbia
  • Miloš B. Simić Center of New Technologies (CNT), Mate Vidakovića 24, 11000 Belgrade, Serbia
  • Dragan D. Manojlović Center of Chemistry, Institute of Chemistry, Technology and Metallurgy (ICTM), University of Belgrade, Njegoševa 12, 11000 Belgrade, Serbia and Faculty of Chemistry, University of Belgrade, Studentski trg 12-16, 11000 Belgrade, Serbia
  • Vesna B. Jović Center of Microelectronic Technologies, Institute of Chemistry, Technology and Metallurgy (ICTM), University of Belgrade – Njegoševa 12, 11000 Belgrade, Serbia

Abstract


 The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM properties show that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard.

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Published
2014/02/10
How to Cite
Dimitrijević, R. Ž., Cvetković, O. G., Miodragović, Z. M., Simić, M. B., Manojlović, D. D., & Jović, V. B. (2013). SEM/EDX AND XRD CHARACTERIZATION OF SILVER NANOCRYSTALLINE THIN FILM PREPARED FROM ORGANOMETALLIC SOLUTION PRECURSOR. Journal of Mining and Metallurgy, Section B: Metallurgy, 49(1), 91. Retrieved from https://aseestant.ceon.rs/index.php/jmm/article/view/2313
Issue
Vol. 49 No. 1 (2013)
Section
Original Scientific Paper

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