Effect of forging sequence and heat treatment on microstructure of high-duty power-plant shaft made of Cr-Mo ultra-high strength steel

Keywords: hot forging, powerplant forged shaft, Cr-Mo high-strength steel AISI 4140, cogging, open-die forging, abnormal grain growth

Abstract


The paper presents the results of modeling and testing of a heavy weight part made of Cr-Mo, which was V-modified ultra-high strength steel grade AISI 4140, processed through a novel open-die forging program and two alternative routes of two-stage heat treatment cycles designed to meet requirements of high-duty components for energy sector. By using unconventional forging conditions based on the assumption of large feed and reduction ratio and modifying the chemical composition, better control of the austenite grain was achieved to minimize abnormal grain growth and/or strain uniformity problems. Using the Finite Element Modeling, the multi-stage sequence of upsetting and the cogging strain distribution were optimized to minimize the strain variation along the length to a range 2.2÷2.7, and correlated with the microstructure generated at each main stage on the large cross-sections of the shaft. Machining cycles designed using the finite element method were fully verified physical modeling using a 16 ton forging block, including two alternative quenching strategies: oil vs. water spray and air. The material was studied in the as-forged, normalized and heat-treated states to observe the behavior of the hot-formed material and the effects of cooling conditions on the microstructure during the final heat treatment. It was found that the use of large feed ratios on cogging and varied cooling allowed to suppress the adverse effects of the inevitable abnormal grain growth, resulting in 1–2 ASTM in forged condition and reaching 6 ASTM and 8/9 ASTM after quenching in oil and water spray, respectively, which allowed a corresponding notched impact strength of 44÷48 and 85÷122 J/cm2 in the critical region of the forged shaft after tempering.

 

Author Biography

Lukasz Lisiecki, AGH University of Science and Technology, Cracow, PL

Faculty of Metals Engineering & Industrial Computer Science,

Adiunct

References

Y. Tanaka, I. Sato, Development of high purity large forgings for nuclear power plants, Journal of Nuclear Materials, 417 (2011) 854–859.


[2]     S.H. Kim, W.S. Ryu, I.H. Kuk, Microstructure and Mechanical Properties of Cr-Mo Steels for Nuclear Industry Applications, Journal of the Korean Nuclear Society, 31 (6) (1999) 561–571.


[3]     K. Suzuki, I. Sato, M. Kusuhashi, H. Tsukada, Current steel forgings and their properties for steam generator of nuclear power plant, Nuclear Engineering and Design, 198 (2000) 15–23.


[4]     A. Pola, M. Gelfi, G.M. La Vecchia, Simulation and validation of spray quenching applied to heavy forgings, Journal of Materials Processing Technology, 213 (2013) 2247–2253.


[5]     G. Quan, Y. Tong, G. Luo, J. Zhou, A characterization for the flow behavior of 42CrMo steel, Computational Materials Science, 50 (2010) 167–171.


[6]     Y.C. Lin, M. S. Chen, J. Zhong,  Effect of temperature and strain rate on the compressive deformation behavior of 42CrMo steel, Journal of Materials Processing Technology, 205 (2008) 308–315.


[7]       E. Kohls, C. Heinzel, M. Eich, Evaluation of Hardness and Residual Stress Changes of AISI 4140 Steel Due to Thermal Load during Surface Grinding, Journal of Manufacturing and Materials Processing, 5 (2021) 73, doi.org/10.3390/jmmp5030073


[8] G. Kang, Y. Liu, J. Ding, Multiaxial ratchetting–fatigue interactions of annealed and tempered 42CrMo steels: Experimental observations, International Journal of Fatigue, 30 (2008) 2104–2118.


[9]     A. Zieliński, J. Dobrzański, H. Krztoń, Structural changes in low alloy cast steel Cr-Mo-V after long time creep service, Journal of Achievements in Materials and Manufacturing Engineering, 25 (1) (2007) 33-36.


[10] L. Keränen, M. Kangaspuoskari, J. Niskanen, Ultrahigh-strength steels at elevated temperatures, Journal of Constructional Steel Research, 183 (2021) 106739


[11] I.A. Borisov, Properties and Defects of Large Forgings, Metal Science and Heat Treatment, 40, (7-8) (1998) 316-318.


[12]   J. Sińczak, J. Majta, M. Głowacki, M. Pietrzyk, Prediction of mechanical properties of heavy forgings, Journal of Materials Processing Technology, 80–81 (1998) 166–173.


[13]   B.A. Marinkovic, R.R. de Avillez, Barros S.K., F.C. Rizzo Assunção, Thermodynamic Evaluation of Carbide Precipitates in 2.25Cr– 1.0Mo Steel for Determination of Service Degradation, Material Research, 5 (4) (2012) 491-495.


[14]   H. Hoseiny, U. Klement, P. Sotskovszki, J. Andersson, Comparison of the microstructures in continuous-cooled and quench-tempered pre-hardened mould steels, Materials and Design, 2 (2011) 21-28.


[15]   Q Ma, Z. Wang, Y. Zhong, The mechanism of faults originating from inclusions in the plastic deformation processes of heavy forging, Journal of Materials Processing Technology, 123 (2002) 61-66.


[16]   Y.S. Lee, S.U. Lee, C.J. Van Tyne, B.D. Joo, Y.H. Moon, Internal void closure during the forging of large cast ingots using a simulation approach, Journal of Materials Processing Technology, 211 (2011) 1136–1145.


[17]   S. Hamzah, U. Stahlberg, A new pore closure concept for the manufacturing of heavy rings. Journal of Materials Processing Technology, 110 (2001) 324-333.


[18]   J. Wang, P. Fu, H. Liu, D. Li, Y. Li, Shrinkage porosity criteria and optimized design of a 100-ton 30Cr2Ni4MoV forging ingot, Materials and Design, 35 (2012) 446-456.


[19]   J.R. Cho, W.B. Bae, Y.H. Kim, S.S. Choi, D.K. Kim, Analysis of the cogging process for heavy ingots by finite element method and physical modelling method, Journal of Materials Processing Technology, 80-81 (1998) 161-165.


[20] W.C. Pei, J.W. Dong, H.C. Ji, H.Y. Long, S.F. Yang, Study on crack propagation in 42CrMo, Metalurgija, 58 (3-4) (2019) 219-222


[21]   ASM Handbook, Nondestructive Evaluation and Quality Control, vol. 17. ASM International Handbook Committee, 1991.


[22]   T.G. Byrer, S.L. Semiatin, D.C. Vollmer, Forging Handbook, Forging Industry Association, American Society of Metals, Cleveland, Ohio, 1985.


[23]   H. Kakimoto, T. Arikawa, Y. Takahashi, T. Tanaka, Y. Imaida, Development of forging process design to close internal voids. Journal of Materials Processing Technology, 210 (2010) 415–422


[24]   J. Pisseloup, P. Bocquet, L. Poitrault, R. Dumont, Optimization of the open die forging of heavy pieces in stainless steel through the control of grain. 14th International Forgemasters Meeting, Wiesbaden, Germany 3-8 (2000) 344-348.


[25]   J. Krawczyk, H. Adrian: The kinetics of austenite grain growth in steel for wind power plant shafts, Archives of Metallurgy and Materials, 55 (1) (2010) 91–99.


[26] H.T. Zhou, H.S. Zuro, Abnormal and post-abnormal austenite grain growth kinetics in Nb-Ti microalloyed steels, Canadian Metallurgical Quarterly, 50 (4) (2011) 389-395


[27] G. Banaszek, A. Stefanik, S. Berski, Computer and Laboratory Modelling of the Analysis of Closing up of Metallurgical Defects In Ingots During Free Hot Forging, Metalurgija,  44 (1) (2005) 25-29.


[28] M. Kukuryk, Experimental and FEM Analysis of Void Closure in the Hot Cogging Process of Tool Steel, Metals, 9 (2019) 538


[29]   L. Zheng, D. Zheng, L. Zhao, L. Wang, K. Zhang, Novel Water-Air Circulation Quenching Process for AISI 4140 Steel, Metals and Materials International, 19 (6) (2013) 1373-1376


[30]   Q Yu, Y. Sun, Abnormal growth of austenite grain of low- carbon steel, Materials Science and Engineering A, 420 (2006) 34 -38.


[31] X.L. Wen, Z. Mei, B. Jiang, L.Ch. Zhang, Y.Z. Liu, Effect of normalizing temperature on microstructure and mechanical properties of a Nb-V microalloyed large forging steel, Materials Science&Engineering A, 671 (2016) 233–243.


[32] A. Brownrigg, G.K. Prior, Hardenability reduction in VN microalloyed eutectoid steels, Scripta Materialia, 46 (2002) 357–361


[33] J.J. Jonas, V.V. Basabe, C. Ghosh,Transformation of Deformed Austenite at Temperatures above the Ae3, Materials Science Forum, 706-709 (2012) 49-54


[34] M. Opiela, W. Zalecki, A. Grajcar, Influence of plastic deformation on CCT-diagrams of new-developed microalloyed steel, Journal of Achievements in Materials and Manufacturing Engineering, 51 (2) (2012) 78-89


[35] A. Fadel, D. Glisic, N. Radovic, D. Drobnjak, Intragranular Ferrite Morphologies in Medium Carbon Vanadium-Microalloyed Steel, Journal of Mining and Metallurgy, Section B: Metallurgy, 49 (3) (2013) 237-244


[36]   P. Skubisz, P. Micek, J. Sińczak, M. Tumidajewicz, Automated determination and on-line correction of emissivity coefficient in controlled cooling of drop forgings, Solid State Phenomena, 177 (2011) 76-83.


[37] J. Pacyna, A. Kokosza, R. Dziurka, Irreversible temper embrittlement, Archives of Materials Science and Engineering, 62 (2) (2013)67-72


[38] H. Adrian, J. Augustyn-Pieniążek, J. Franek, M. Osika, P. Marynowski, Analiza współczynnika przejmowania ciepła wybranych olejów hartowniczych (Analysis of the heat transfer coefficient of selected quenching oils), Hutnik - Wiadomości Hutnicze, 80 (4) (2013) 267–273 (in Polish).


[39] M. Apostoł; P. Skubisz, H. Adrian, Determination of Heat Transfer Coefficient for Air-Atomized Water Spray Cooling and Its Application in Modeling of Thermomechanical Controlled Processing of Die Forgings, Materials, 15 (2022) 2366.


[40] V.A. Shamrei, S.I. Zhul’ev, New Shape of Forging Ingot for Making Hollow Forged Products, Metallurgist, 51 (11–12) (2007) 617-623.


[41] P. Skubisz, J. Sińczak, Ł. Lisiecki, Studies of the quality and cost-effectiveness of a novel concept of open-die forged powerplant main shaft, Metalurgija, 54 (2) (2015) 339-342.


[42] P. Kawulok, P. Opela, I. Schindler, R. Kawulok, S. Rusz, M. Sauer, K. Konecná, Hot Deformation Behavior of Non-Alloyed Carbon Steels, Materials, 15 (2022) 595, https://doi.org/10.3390/ma15020595


[43] I. Olejarczyk-Wożeńska, H. Adrian, B. Mrzygłód, Mathematical model of the process of pearlite austenitization, Archives of Metallurgy and Materials, 59 (3) (2014) 981–986.


[44] L. Rausa, J. Ďurica, M. Martinkovic, R. Čicka, M. Pasak, P. Jurci, The influence of austenitizing temperature level on microstructure development in chromium ledeburitic tool steel, Proceedings of conf. Metal, May 26 - 28, 2021, Brno, Czech Republic.


[45]   D.C. Wen: Effect of Prior Hot Rolling on the Microstructures and Mechanical Properties of Duplex Stainless Steel Containing Tempered Martensite and Ferrite, Metals and Materials International, 15 (3) (2009) 365-372.

Published
2023/12/01
How to Cite
Skubisz, P., & Lisiecki, L. (2023). Effect of forging sequence and heat treatment on microstructure of high-duty power-plant shaft made of Cr-Mo ultra-high strength steel . Journal of Mining and Metallurgy, Section B: Metallurgy, 59(2), 299-314. Retrieved from https://aseestant.ceon.rs/index.php/jmm/article/view/40517
Section
Original Scientific Paper