Influence of thermal ageing on tensile-plastic flow and work hardening parameters of Indian reduced activated ferritic martensitic steel

  • Kanhu Charan Sahoo HBNI, Mumbai
  • Kinkar Laha Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research Kalpakkam
Keywords: Indian Reduced Activated Ferritic Martensitic steel, Thermal ageing, microscopy studies, Tensile-plastic flow behaviour, Ludwigson and Voce relation

Abstract


The present study investigates the influence of thermal ageing (873K/5000h) on the microstructure, tensile-plastic flow behavior, and work hardening parameters of normalized and tempered (N&T) 1.4W-0.06Ta Indian Reduced Activated Ferritic Martensitic (INRAFM) steel. To comprehensively understand the tensile-plastic flow response of the INRAFM steel across a broad temperature spectrum of 300-873 K, the Hollomon, Ludwigson and Voce equations were employed. The results reveal an augmentation in the strain hardening exponent following the ageing process, attributed to the heightened work hardening capability of the aged steel, while the strain hardening coefficient exhibited a decline post ageing. To elucidate the dislocation debris structure's formation and movement within both the N&T and thermally aged specimens, transmission electron microscopy (TEM) specimens were procured in close proximity to the tensile tested specimens at varying temperatures of 300, 573 and 873 K. The tensile plastic flow behavior at diverse temperatures was aptly described by Hollomon, Ludwigson, and Voce equations. The fitting accuracy of these equations was determined using the goodness of fit, as indicated by the lowest χ2 values. The constitutive Voce equation successfully captured the yield strength (YS) and ultimate tensile strength (UTS) with the initial stress and saturation stress acting as fitting parameters. Distinct patterns of initial stress and saturation stress variations were observed concerning both N&T and aged steel in relation to temperature. Furthermore, absolute value of the Voce strain component (nv) demonstrated a reduction consequent to ageing, manifesting a two-stage behavior corresponding to temperature elevation. Notably, the deceleration of the recovery process during high temperature conditions was more pronounced in the thermally aged steel when contrasted with the N&T steel. Conclusively, the Voce relation proved efficacious in predicting the yield stress (YS) and ultimate tensile strength (UTS) of both the thermally aged and N&T INRAFM steel at varying temperatures.

 

References

1. The ITER project. EFDA, European Fusion Development Agreement (2006).

2. D. M. Meade; Tokamak Fusion Test Reactor D-T results, Fusion Engineering Design, 30, (1995) 13-23. https://doi.org/10.1016/0920-3796(94)00398-Q

3. P. Rodriguez, R. Krishnan, C.V. Sundaram; Radiation effects in nuclear reactor materials-correlation with structure, Bulletin Material Science, 6 (1984) 339–367. https://doi.org/10.1007/BF02743907

4. B. Raj, T. Jayakumar; Development of Reduced Activation Ferritic–Martensitic Steels and fabrication technologies for Indian test blanket module, Journal of Nuclear Material, 417 (2011). 72–76.  https://doi.org/10.1016/j.jnucmat.2011.02.032

5. R. L. Klueh, E. E Bloom., The development of ferritic steels for fast induced-radioactivity decay for fusion reactor applications, Nuclear Engineering and Design, 2 383–389 (1985). https://doi.org/10.1016/0167-899X(85)90026-6" target="_blank" rel="noopener">https://doi.org/10.1016/0167-899X(85)90026-6 style="font-size: 12.0pt; font-family: 'Times New Roman','serif'; color: black; mso-themecolor: text1;">.

6. R. Lindau R., M. Schirran First results on the characterisation of the reduced-activation-ferritic-martensitic steel EUROFER, Fusion Engineering and Design, 58-59 (2001) 781–785. https://doi.org/10.1016/S0920-3796(01)00562-2" target="_blank" rel="noopener">https://doi.org/10.1016/S0920-3796(01)00562-2>

7. A. Alamo, J. C. Brachet, A. Castaing, C. Lepoittevin, and F. Barcelo, Physical metallurgy and mechanical behaviour of FeCrWTaV low activation martensitic steels: Effects of chemical composition, Journal of Nuclear Material, 258–263 (1998) 1228–1235. https://doi.org/10.1016/S0022-3115(98)00190-1" target="_blank" rel="noopener">https://doi.org/10.1016/S0022-3115(98)00190-1>

8. R. L. Klueh and M. A. Sokolov; Mechanical properties of irradiated 9Cr–2WVTa steel with and without nickel, Journal of Nuclear Material, 367 (2007) 102-106. https://doi.org/10.1016/j.jnucmat.2007.03.160" target="_blank" rel="noopener">https://doi.org/10.1016/j.jnucmat.2007.03.160 style="font-size: 12.0pt; font-family: 'Times New Roman','serif'; color: black; mso-themecolor: text1;">.

9. E. Wakai, M. Sato, T. Sawai, K. Shiba and S. Jitsukawa; Mechanical Properties and Microstructure of F82H Steel doped with Boron or Boron and Nitrogen as a Function of Heat Treatment, Materials Transaction, 45 (2004) 407-410. https://doi.org/10.2320/matertrans.45.407

10. K. Mergia, N. Boukos; Structural, thermal, electrical and magnetic properties of Eurofer 97 steel; Journal of Nuclear Material, 373 (2008) 1-8. https://doi.org/10.1016/j.jnucmat.2007.03.267

11. J. H. Hollomon; Tensile deformation, Transaction AIME, 162 (1945) 268-290.

12. D. C. Ludwigson; Modified stress-strain relation for FCC metals and alloys, Metallurgical Transaction, 2 (1971) 2825–2828. https://doi.org/10.1007/BF02813258

13. E. Voce; The relationship between stress and strain for homogeneous deformation, Journal of Institute of Metal, 74 (1948) 537–562. https://cir.nii.ac.jp/crid/1573950400805224960

14. E. Voce; A practical strain hardening function, Metallurgia, 51 (1955) 219–226. https://cir.nii.ac.jp/crid/1573668925830119040.

15. K. C. Sahoo, J. Vanaja, P. Parameswaran, V. D. Vijayanand, K. Laha; Effect of thermal ageing on microstructure, tensile and impact properties of reduced activated ferritic-martensitic steel, Material Science & Engineering A, 686 (2017) 54–64.  https://doi.org/10.1016/j.msea.2017.01.030" target="_blank" rel="noopener">https://doi.org/10.1016/j.msea.2017.01.030>

16. A. Moitra, P. R. Sreenivasan, P. Parameswaran, S. L. Mannan; Dynamic deformation and fracture properties of simulated weld heat affected zone of 9Cr-1Mo steel from instrumented impact tests, Material Science and Technology, 18 (2002) 1195-1200. https://doi.org/10.1179/026708302225006106.

17. A. Ghosh, A. Ray, D. Chakrabarti, C. L. Davis; Cleavage initiation in steel: Competition between large grains and large particles, Material Science & Engineering A, 561 (2013) 126–135. https://doi.org/10.1016/j.msea.2012.11.019.

18. R.W. Hayes, W.C. Hayes; A proposed model for the disappearance of serrated flow in two Fe alloys, Acta Metallurgica, 32 (1984) 259–267. https://doi.org/10.1016/0001-6160(84)90054-3" target="_blank" rel="noopener">https://doi.org/10.1016/0001-6160(84)90054-3 style="font-size: 12.0pt; font-family: 'Times New Roman','serif'; color: black; mso-themecolor: text1;">.

19. H. Mecking, U.F. Kocks; Kinetics of flow and strain-hardening, Acta Metallurgical and Materials, 29 (1981) 1865–1875. https://doi.org/10.1016/0001-6160(81)90112-7" target="_blank" rel="noopener">https://doi.org/10.1016/0001-6160(81)90112-7 style="font-size: 12.0pt; font-family: 'Times New Roman','serif'; color: black; mso-themecolor: text1;">.

20. Y. Estrin, H. Mecking; A unified phenomenological description of work hardening and creep based on one-parameter models, Acta Metallurgical and Materials, 32 (1984) 57–70. https://doi.org/10.1016/0001-6160(84)90202-5" target="_blank" rel="noopener">https://doi.org/10.1016/0001-6160(84)90202-5 style="font-size: 12.0pt; font-family: 'Times New Roman','serif'; color: black; mso-themecolor: text1;">.

21. N.S. Mishra, Sanak Mishra, V. Ramaswamy; Analysis of the temperature dependence of strain-hardening behavior in high-strength steel, Metallurgical Transaction A, 20 (1989) 2819–2829. https://doi.org/10.1007/BF02670174.

Published
2023/12/01
How to Cite
Sahoo, K. C., & Laha, K. (2023). Influence of thermal ageing on tensile-plastic flow and work hardening parameters of Indian reduced activated ferritic martensitic steel. Journal of Mining and Metallurgy, Section B: Metallurgy, 59(2), 217-229. Retrieved from https://aseestant.ceon.rs/index.php/jmm/article/view/41164
Section
Original Scientific Paper