Effect of reduction ratio on die fill-out and hardness profile of cold-drawn polygonal rods made of acid resistant steel X6CrNiTi18-10
Abstract
The study investigates the effect of the reduction ratio on strain hardening efficiency and load during the drawing process of austenitic acid-resistant steel X6CrNiTi18-10. The focus is on optimizing geometry-related process conditions to achieve the highest quality and productivity when drawing special-purpose rods with polygonal shapes, specifically square and hexagonal cross-sections. The research addresses how increasing the reduction ratio can enhance strain hardening while reducing the number of drawing passes, ultimately affecting quality and load. Numerical modeling was used to analyze the relationship between strain hardening and load versus the reduction ratio. Proper models and assumptions were formulated and subsequently verified through experiments, which confirmed the validity of the mathematical and numerical models for load estimation. The study quantified the effect of strain on strength properties by mapping of measured hardness along the strain gradient. The application of variable billet diameters produced a similar hardness profiles for both analyzed rod geometries and reversed the effect on underfilling of the corners. The findings indicate a threshold reduction ratio for producing sound rods with square or hexagonal cross-sections. Exceeding this threshold can cause excessive strain hardening, leading to increased hardness that impedes corner fill-out and/or results in failure.
References
[2] D. Bricín and H. Gilík, “Surface Structure Analysis of X12CrNiMoV12-3 and X6CrNiTi18-10 Steel Samples Processed by Laser Shot Peening (LSP),” MATEC Web Conf., vol. 367, p. 00004, 2022, doi: 10.1051/matecconf/202236700004.
[3] E. Kantoríková, “An Influence of Nitrogen Corrosion on Microstructural and Mechanical Features of the X5CrNi18-10 Steel,” vol. 24, no. 3, pp. 69–75, 2024, doi: 10.24425/afe.2024.151293.
[4] L. Donati, B. Reggiani, R. Pelaccia, M. Negozio, and S. Di Donato, “Advancements in extrusion and drawing: a review of the contributes by the ESAFORM community,” Int. J. Mater. Form., vol. 15, no. 3, 2022, doi: 10.1007/s12289-022-01664-w.
[5] J. H. Kim, J. H. Park, K. S. Lee, D. C. Ko, and K. H. Lee, “Design of an Intermediate Die for the Multi-Pass Shape Drawing Process,” Materials (Basel)., vol. 15, no. 19, 2022, doi: 10.3390/ma15196893.
[6] K. M. W. Głuchowski, J. Domagała-Dubiel, J. Sobota, Z. Rdzawski, J. Stobrawa, “Analiza procesu ciągnienia drutów Cu-Ag,” vol. 18, no. 8, pp. 530–533, 2013, [Online Available: YADDA bwmeta1.element.baztech-31f3a807-1979-4c71-a411-77e2d865ad17]
[7] A. Sasaki, M. Nakano, H. Takao, and H. Utsunomiya, “Pass-Schedule Design for Non-circular Wire Drawing,” Lect. Notes Mech. Eng., vol. 1, pp. 407–417, 2024, doi: 10.1007/978-3-031-41023-9_42.
[8] S.K. Lee, I.K. Lee, S.M. Lee, and S.Y. Lee, “Prediction of Effective Strain Distribution in Two-Pass Drawn Wire,” Materials, vol. 12, 3923; 2019, doi:10.3390/ma12233923.
[9] S. Di Donato, M. Negozio, R. Pelaccia, B. Reggiani, and L. Donati, “Experimental, analytical, and numerical analysis of the copper wire multi-pass drawing process,” Mater. Res. Proc., vol. 41, no. April, pp. 742–752, 2024, doi: 10.21741/9781644903131-82.
[10] S. Alexandrov, Y. M. Hwang, and H. S. R. Tsui, “Determining the Drawing Force in a Wire Drawing Process Considering an Arbitrary Hardening Law,” Processes, vol. 10, no. 7, 2022, doi: 10.3390/pr10071336.
[11] S. H. Zhang, X. D. Chen, J. Zhou, and D. W. Zhao, “Upper bound analysis of wire drawing through a twin parabolic die,” Meccanica, vol. 51, no. 9, pp. 2099–2110, 2016, doi: 10.1007/s11012-016-0363-9.
[12] R. Badi, S. Bensaada, N. Tala-Ighil, and N. Lebaal, “Numerical analysis of the effects of incremental reduction rate in the wire drawing process,” Int. J. Adv. Manuf. Technol., vol. 133, no. 11–12, pp. 5197–5209, 2024, doi: 10.1007/s00170-024-13982-1.
[13] I. Kacar and S. Yildirim, “Parameter Calibration of a Novel Combined Hardening Model for a Wire Drawing Simulation of AA7075-T6,” J. Mater. Eng. Perform., 2024, doi: 10.1007/s11665-024-10377-x.
[14] A. Whelan, T. Tang, V. Pakrashi, and P. Cardiff, “A Finite Volume Framework for Damage and Fracture Prediction in Wire Drawing,” Int. J. Numer. Methods Eng., vol. 126, no. 1, 2025, doi: 10.1002/nme.7640.
[15] F. J. Doblas-Charneco, D. Morales-Palma, A. Estévez, and C. Vallellano, “Mathematical optimization of cold wire drawing operations,” Adv. Sci. Technol., vol. 132 AST, pp. 13–21, 2023, doi: 10.4028/p-3lhBRy.
[16] T. G. dos Santos et al., “Experimental-numerical analysis to determine the efficiency of industrial lubricants in wire drawing process,” Rev. Metal., vol. 59, no. 1, pp. 1–10, 2023, doi: 10.3989/revmetalm.234.
[17] E. Ruiz, M. Cuartas, D. Ferreno, L. Romero, V. Arroyo, and F. Gutierrez-Solana, “Optimization of the fabrication of cold drawn steel wire through classification and clustering machine learning algorithms,” IEEE Access, vol. 7, pp. 141689–141700, 2019, doi: 10.1109/ACCESS.2019.2942957.
[18] R. J. Kuo and Z. X. Xu, “Predictive maintenance for wire drawing machine using MiniRocket and GA-based ensemble method,” Int J Adv Manuf Technol, vol. 134, no. 3–4, pp. 1661–1676, 2024, doi: 10.1007/s00170-024-14225-z.
[19] P. Kumar and G. Agnihotri, “Cold drawing process - A review Cold Drawing Process”, Int J Eng Res Appl, vol. 3, iss. 3, 2013, pp.988-994
[20] L. V. Radionova, D. V. Gromov, R. A. Lisovskiy and I. N. Erdakov, “Experimental Determination and Calculation of the Wire Drawing Force in Monolithic Dies on Straight-Line Drawing Machines,” Machines, vol. 11, no. 2, pp. 1–13, 2023, doi: 10.3390/machines11020252.
[21] L. Sadok, M. Packo, A. Skolyszewski, and M. Ruminski, “Influence of the shape of the die on the field of strains in the drawing process,” J Mater Process Tech, vol. 34, no. 1–4, pp. 381–388, 1992, doi: 10.1016/0924-0136(92)90131-B.
[22] P. Gawali and N. Gautam, “Variation in mechanical properties of wire due to variation of speed in wire drawing process”. Journal of Emerging Technologies and Innovative Research, vol. 9 , iss.12, 2022, pp. 5–11,
[23] L. V. Radionova, R. A. Lisovskiy, A. S. Svistun, D. V. Gromov, and I. N. Erdakov, “FEM Simulation Analysis of Wire Drawing Process at Different Angles Dies on Straight-Line Drawing Machines,” Lect. Notes Mech. Eng., 8th International Conference on Industrial Engineering, ICIE 16-20 May 2022, online, Springer Science and Business Media Deutschland GmbH, pp. 769–778, 2023, doi: 10.1007/978-3-031-14125-6_75.
[24] S. Y. Lee, I. K. Lee, S. K. Lee, S. K. Hwang, and D. Park, “Fabrication of 30.0 μm fine rhodium wire from 80.0 μm initial wire using multi-pass wire drawing process,” J. Mech. Sci. Technol., vol. 35, no. 6, pp. 2637–2644, 2021, doi: 10.1007/s12206-021-0534-z.
[25] S. Verma and P.S. Rao, “Multistage wire-drawing process analysis and optimization of process parameters. Int. J. Tech. Innov. Mod. Eng. Sci.,” vol. 5, iss. 01, 2019, pp. 173-183.
[26] S. Wiewiórowska and Z. Muskalski, “The influnece of the partial single reduction on mechanical properties wires made from trip steel with 0,43% C,” Metalurgija, vol. 54, no. 1, pp. 184–186, 2015.
[27] S.K. Lee, I.K. Lee, S. Y. Lee, M. S. Jeong, Y. H. Moon and S. K. Lee “Evaluation of Radial Direction Non-uniform Strain in Drawn Bar,” Transactions of Materials Processing, vol. 29, no. 6, 2020, doi: 10.5228/KSTP.2020.29.6.356.
[28] Á. González, M. Cruchaga, D. Celentano, and J. P. Ponthot, “Damage Prediction in the Wire Drawing Process,” Metals (Basel)., vol. 14, no. 10, pp. 1–16, 2024, doi: 10.3390/met14101174.
[29] M. Suliga, P. Szota, M. Gwoździk, J. Kulasa, and A. Brudny, “The Influence of Temperature in the Wire Drawing Process on the Wear of Drawing Dies,” Materials, vol. 17, no. 20, 2024, doi: 10.3390/ma17204949.
[30] S. Wiewiórowska, “Analysis of the influence of drawing process parameters on the mechanical properties of trip-structure steel wires,” Arch. Metall. Mater., vol. 58, no. 2, pp. 573–578, 2013, doi: 10.2478/amm-2013-0040.
[31] P. Skubisz, M. Rumiński, and Ł. Lisiecki, “Estimation of Strain-Hardness Correlation in Cold-Forged Austenitic Stainless Steel,” Key Eng. Mater., Sep. 2014, doi: 10.4028/www.scientific.net/kem.622-623.179.
[32] J. Toribio and M. Lorenzo, “Influence of the Straining Path during Cold Drawing on the Hydrogen Embrittlement of Prestressing Steel Wires,” Metals (Basel)., vol. 13, no. 7, 2023, doi: 10.3390/met13071321.
[33] W. He, F. Li, H. Zhang, H. Chen, and H. Guo, “The influence of cold rolling deformation on tensile properties and microstructures of Mn18Cr18 N austenitic stainless steel,” Mater. Sci. Eng. A, vol. 764, no. April, p. 138245, 2019, doi: 10.1016/j.msea.2019.138245.
[34] I. Kniazkin et al., “Investigation of the skin contamination predictability by means of QForm UK extrusion code,” Mater. Res. Proc., vol. 28, no. February 2024, pp. 543–552, 2023, doi: 10.21741/9781644902479-59.
Authors retain copyright of the published papers and grant to the publisher the non-exclusive right to publish the article, to be cited as its original publisher in case of reuse, and to distribute it in all forms and media.
The Author(s) warrant that their manuscript is their original work that has not been published before; that it is not under consideration for publication elsewhere; and that its publication has been approved by all co-authors, if any, as well as tacitly or explicitly by the responsible authorities at the institution where the work was carried out. The Author(s) affirm that the article contains no unfounded or unlawful statements and does not violate the rights of others. The author(s) also affirm that they hold no conflict of interest that may affect the integrity of the Manuscript and the validity of the findings presented in it. The Corresponding author, as the signing author, warrants that he/she has full power to make this grant on behalf of the Author(s). Any software contained in the Supplemental Materials is free from viruses, contaminants or worms.The published articles will be distributed under the Creative Commons Attribution ShareAlike 4.0 International license (CC BY-SA).
Authors are permitted to deposit publisher's version (PDF) of their work in an institutional repository, subject-based repository, author's personal website (including social networking sites, such as ResearchGate, Academia.edu, etc.), and/or departmental website at any time after publication.
Upon receiving the proofs, the Author(s) agree to promptly check the proofs carefully, correct any typographical errors, and authorize the publication of the corrected proofs.
The Corresponding author agrees to inform his/her co-authors, of any of the above terms.
