A comparative study of mechanical behaviour of heat-treated 3D printed In-718 and ASTM F75 alloys across multiple length scales

  • Muhammad Zubair University of Engineering and Technology Lahore, Pakistan https://orcid.org/0000-0002-1817-7432
  • Khushnuda Nur University of Engineering and Technology Lahore, Pakistan https://orcid.org/0000-0001-5460-641X
  • Ehsan ul Haq University of Engineering and Technology Lahore, Pakistan https://orcid.org/0000-0003-1564-7264
  • Furqan Ahmed University of Engineering and Technology Lahore, Pakistan https://orcid.org/0000-0001-5971-4946
  • Muhammad Adil Javed IMMESNA, Dubai, UAE
  • Muhammad Junaid Khan University of Engineering and Technology Lahore, Pakistan
  • Muhammad Mubeen Naveed University of Engineering and Technology Lahore, Pakistan
  • Mirza Mueed ul Hassan University of Engineering and Technology Lahore, Pakistan
  • Ahmed Abdullah University of Engineering and Technology Lahore, Pakistan
Keywords: Mechanical properties, Nanoindentation, Mechanical behaviour, Alloys

Abstract


The hardness and strength of many alloys often differ when measured at the nano, micro, and macroscopic scales. Therefore, it is essential to study the mechanical behavior of important alloys across a wide range of length scales. In this work, we present a scenario in which two industrially significant alloys, In-718 and ASTM F75, exhibit different behaviors at the micro and macroscopic levels. Both alloys are promising candidates for similar applications in the aerospace and petroleum industries. The alloys were first 3D printed using selective laser melting (SLM) and then heat-treated in a vacuum. The average yield strength and percentage elongation (along the build direction) of the In-718 alloy were 29% and 19% higher, respectively, than those observed for the ASTM F75 alloy. The difference between the ultimate tensile strength (UTS) and Vickers hardness (at a load of 98 N) was almost negligible, i.e., less than 5%. In contrast to the Vickers hardness values of 3.9 GPa and 3.8 GPa, the average nanohardness of the In-718 and ASTM F75 alloys was 5.7 GPa and 7.6 GPa, respectively, which was substantially higher than their Vickers hardness. Furthermore, the ASTM F75 alloy demonstrated much better wear resistance in ScanningWear tests performed using a nanoindenter. The explanation for these differences and the similarities between macro- and nanomechanical behavior are presented in this work.

 

Author Biographies

Muhammad Zubair, University of Engineering and Technology Lahore, Pakistan

Assistant Professor, Department of Metallurgical and Materials Engineering, UET Lahore, Pakistan

Khushnuda Nur, University of Engineering and Technology Lahore, Pakistan

Assistant Professor, Department of Metallurgical and Materials Engineering, UET Lahore, Pakistan

Ehsan ul Haq, University of Engineering and Technology Lahore, Pakistan

Associate Professor, Department of Metallurgical and Materials Engineering, UET Lahore, Pakistan

Furqan Ahmed, University of Engineering and Technology Lahore, Pakistan

Professor, Department of Metallurgical and Materials Engineering, UET Lahore, Pakistan

References

T. Sonar, V. Balasubramanian, S. Malarvizhi, T. Venkateswaran, D. Sivakumar, An overview on welding of Inconel 718 alloy - Effect of welding processes on microstructural evolution and mechanical properties of joints, Materials Characterization, 174 (2021) 110997. https://doi.org/10.1016/j.matchar.2021.110997

M. Shahwaz, P. Nath, I. Sen, A critical review on the microstructure and mechanical properties correlation of additively manufactured nickel-based superalloys, Journal of Alloys and Compounds, 907 (2022) 164530. https://doi.org/10.1016/j.jallcom.2022.164530

H.K.D.H. Bhadeshia, Nickel Based Superalloys, Available at: https://www.phasetrans. msm.cam.ac.uk/2003/Superalloys/superalloys.ht ml

H. Wang, A. Dhiman, H.E. Ostergaard, Y. Zhang, T. Siegmund, J.J. Kruzic, V. Tomar, Nanoindentation based properties of Inconel 718 at elevated temperatures: A comparison of conventional versus additively manufactured samples, International Journal of Plasticity, 120 (2019) 380-394. https://doi.org/10.1016/j.ijplas.2019.04.018

M. Choi, H. Lee, Y. Song, J. Kim, J. Gwon, H. N. Han, B. Lee, Correlation between microstructures and mechanical properties in directly deposited Co-Cr-Mo alloys with line energies, Materials Characterization, 213 (2024) 113994. https://doi.org/10.1016/j.matchar.2024.113994

H.-T. Im, D.H. Kim, Y.D. Kim, J.O. Fadonougbo, C.B. Mo, J.-Y. Park, K.B. Park, J.-W. Kang, H.-S. Kang, H.- K. Park, Effect of phase transformation on the mechanical properties of the Co-Cr-Mo alloy fabricated by selective laser melting, Materials Characterization, 186 (2022) 111767. https://doi.org/10.1016/j.matchar.2022.111767

J. Quintero-Ortiz, F.V. Guerra, A. Bedolla-Jacuinde, C. A. Leon-Patiño, J.S. Pacheco-Cedeño, Sliding wear behavior of Co-Cr-Mo alloys with C and B additions for wear applications, Wear, 522 (2023) 204698. https://doi.org/10.1016/j.wear.2023.204698

M. Atapour, S. Sanaei, Z. Wei, M. Sheikholeslam, J.D. Henderson, U. Eduok, Y. K. Hosein, D.W. Holdsworth, Y.S. Hedberg, H.R. Ghorbani, In vitro corrosion and biocompatibility behavior of CoCrMo alloy manufactured by laser powder bed fusion parallel and perpendicular to the build direction, Electrochimica Acta, 445 (2023) 142059. https://doi.org/10.1016/j.electacta.2023.142059

K. Zhou, J. Chen, T. Wang, Y. Su, L. Qiao, Y. Yan, Effect of surface energy on protein adsorption behaviours of treated CoCrMo alloy surfaces, Applied Surface Science, 520 (2020) 146354. https://doi.org/10.1016/j.apsusc.2020.146354

J.V. Giacchi, O. Fornaro, H. Palacio, Microstructural evolution during solution treatment of Co–Cr–Mo–C biocompatible alloys, Materials Characterization, 68 (2012) 49-57. https://doi.org/10.1016/j.matchar.2012.03.006

S.L. Sing, S. Huang, W.Y. Yeong, Effect of solution heat treatment on microstructure and mechanical properties of laser powder bed fusion produced cobalt- 28chromium-6molybdenum, Materials Science and Engineering: A, 769 (2020) 138511. https://doi.org/10.1016/j.msea.2019.138511

G. Cui, H. Liu, S. Li, G. Gao, M. Hassani, Z. Kou, Effect of Ni, W and Mo on the microstructure, phases and high-temperature sliding wear performance of CoCr matrix alloys, Science and Technology of Advanced Materials, 21 (1) (2020) 229-241. https://doi.org/10.1080/14686996.2020.1752113

O. Franke, J.C. Trenkle, C.A. Schuh, Temperature dependence of the indentation size effect, Journal of Materials Research, 25 (7) (2010) 1225-1229. https://doi.org/10.1557/JMR.2010.0159

V. Maier, C. Schunk, M. Göken, K. Durst, Microstructure-dependent deformation behaviour of bcc-metals – indentation size effect and strain rate sensitivity, Philosophical Magazine, 95 (16-18) (2015) 1766-1779. https://doi.org/10.1080/14786435.2014.982741

W.D. Nix, H. Gao, Indentation size effects in crystalline materials: A law for strain gradient plasticity, Journal of the Mechanics and Physics of Solids, 46 (3) (1998) 411-425. https://doi.org/10.1016/S0022-5096(97)00086-0

M. Zubair, S. Sandlöbes-Haut, M. Lipińska-Chwałek, M.A. Wollenweber, C. Zehnder, J. Mayer, J.S.K.L. Gibson, S. Korte-Kerzel, Co-deformation between the metallic matrix and intermetallic phases in a creepresistant Mg-3.68Al-3.8Ca alloy, Materials & Design, 210 (2021) 110113. https://doi.org/10.1016/j.matdes.2021.110113

P. Wang, Y. Gao, P. Wang, A comparative study of indentation size effect models for different materials, Scientific Reports, 14 (1) (2024) 20010. https://doi.org/10.1038/s41598-024-71136-5

R. Jiang, A. Mostafaei, Z. Wu, A. Choi, P.-W. Guan, M. Chmielus, A.D. Rollett, Effect of heat treatment on microstructural evolution and hardness homogeneity in laser powder bed fusion of alloy 718, Additive Manufacturing, 35 (2020) 101282. https://doi.org/10.1016/j.addma.2020.101282

S. Naskar, S. Suryakumar, B.B. Panigrahi, Heat treatments effects on wear performance of laser based powder bed dusion fabricated Inconel 718 alloy, Wear, 556-557 (2024) 205526. https://doi.org/10.1016/j.wear.2024.205526

V.K.A, P. K.R, H.P, J.K. Katiyar, S.K, Advancements in laser powder bed fusion manufacturing of Alloy 718: Microstructural insights and mechanical behaviours, Journal of Alloys and Compounds, 1037 (2025) 182631. https://doi.org/10.1016/j.jallcom.2025.182631

M.E. Korkmaz, M.K. Gupta, G. Robak, K. Moj, G.M. Krolczyk, M. Kuntoğlu, Development of lattice structure with selective laser melting process: A state of the art on properties, future trends and challenges, Journal of Manufacturing Processes, 81 (2022) 1040- 1063. https://doi.org/10.1016/j.jmapro.2022.07.051

L. Xu, Z. Chai, B. Peng, W. Zhou, X. Chen, Effect of heat treatment on microstructures and mechanical properties of Inconel 718 additively manufactured using gradient laser power, Materials Science and Engineering: A, 868 (2023) 144754. https://doi.org/10.1016/j.msea.2023.144754

M. Švec, P. Solfronk, I. Nováková, J. Sobotka, J. Moravec, Comparison of the structure, mechanical properties and effect of heat treatment on alloy Inconel 718 produced by conventional technology and by additive layer manufacturing, Materials, 16 (15) (2023) 5382. https://doi.org/10.3390/ma16155382

H. Deng, Y. Wang, L. Lv, S. Zhang, Q. Bian, J. Luo, Z. Wu, Z. Liu, Z. Chen, L. Tan, F. Liu, Orientation dependence of microstructure and mechanical property in selective laser-melted Inconel 718 alloy, Materials Characterization, 220 (2025) 114664. https://doi.org/10.1016/j.matchar.2024.114664

S.N. Emmanouilidou, A.G. Lekatou, A.D. Papagiannopoulos, Z.Z. Siaraka, I.E. Tzala, Effect of Nb low-alloying on the microstructure, corrosion and wear performance of a Co-28Cr-6Mo alloy fabricated by vacuum arc melting, International Journal of Refractory Metals and Hard Materials, 133 (2025) 107330. https://doi.org/10.1016/j.ijrmhm.2025.107330

W.C. Oliver, G.M. Pharr, Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology, Journal of Materials Research, 19 (1) (2004) 3-20. https://doi.org/10.1557/jmr.2004.19.1.3

W.C. Oliver, G.M. Pharr, An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments, Journal of Materials Research, 7 (6) (1992) 1564-1583. https://doi.org/10.1557/JMR.1992.1564

J. Zhao, L. Sun, P. Ji, X. Yu, L. Chen, S. Liu, K. Zheng, F. Yin, The effect of scanning strategies on the microstructure and mechanical properties of M2052 alloy manufactured by selective laser melting, Journal of Materials Research and Technology, 27 (2023) 7084-7093. https://doi.org/10.1016/j.jmrt.2023.11.141

V.G. Efremenko, A.G. Lekatou, Y.G. Chabak, B.V. Efremenko, I. Petryshynets, V.I. Zurnadzhy, S. Emmanouilidou, M. Vojtko, Micromechanical, corrosion and wet sliding wear behaviours of Co-28Cr- 6Mo alloy: Wrought vs. LPBF, Materials Today Communications, 35 (2023) 105936. https://doi.org/10.1016/j.mtcomm.2023.105936

J.J. Shi, Z.Q. Zhou, K. Xu, G.Y. Zhou, Z.J. Zhou, C.P. treatment on microstructure and small punch creep property of selective laser melted Inconel 718 alloy, Materials Science and Engineering: A, 853 (2022) 143748. https://doi.org/10.1016/j.msea.2022.143748

V.K. Singh, D. Sahoo, M. Amirthalingam, S. Karagadde, S.K. Mishra, Dissolution of the Laves phase and δ-precipitate formation mechanism in additively manufactured Inconel 718 during post printing heat treatments, Additive Manufacturing, 81 (2024) 104021. https://doi.org/10.1016/j.addma.2024.104021

N. Li, C. Wang, C. Li, Microstructures and hightemperature mechanical properties of Inconel 718 superalloy fabricated via laser powder bed fusion, Materials, 17 (15) (2024) 3735. https://doi.org/10.3390/ma17153735

M. Sundararaman, P. Mukhopadhyay, S. Banerjee, Precipitation of the δ-Ni3Nb phase in two nickel base superalloys, Metallurgical Transactions A, 19 (3) (1988) 453-465. https://doi.org/10.1007/BF02649259

K.M. Mantrala, M. Das, V.K. Balla, C.S. Rao, V.V.S. Kesava Rao, Additive manufacturing of Co-Cr-Mo alloy: Influence of heat treatment on microstructure, tribological, and electrochemical properties, Frontiers in Mechanical Engineering, 1 (2015) 1-7. https://doi.org/10.3389/fmech.2015.00002

E. Bettini, C. Leygraf, C. Lin, P. Liu, J. Pan, Influence of grain boundaries on dissolution behavior of a biomedical CoCrMo alloy: In-situ electrochemicaloptical, AFM and SEM/TEM studies, Journal of The Electrochemical Society, 159 (9) (2012) C422-C427. https://doi.org/10.1149/2.056209jes

T.-N. Lam, K.-M. Chen, C.-H. Tsai, P.-I. Tsai, M.-H. Wu, C.-C. Hsu, J. Jain, E. W. Huang, Effect of porosity and heat treatment on mechanical properties of additive manufactured CoCrMo Alloys, Materials, 16 (2) (2023) 751. https://doi.org/10.3390/ma16020751

M. Roudnicka, J. Bigas, O. Molnarova, D. Palousek, D. Vojtech, Different response of cast and 3D-printed Co- Cr-Mo alloy to heat treatment: A thorough microstructure characterization, Metals, 11 (5) (2021) 687. https://doi.org/10.3390/met11050687

Y. Wang, J. Shi, Recrystallization behavior and tensile properties of laser metal deposited Inconel 718 upon in-situ ultrasonic impact peening and heat treatment, Materials Science and Engineering: A, 786 (2020) 139434. https://doi.org/10.1016/j.msea.2020.139434

L. Zhu, Z. Xu, Y. Gu, Effect of laser power on the microstructure and mechanical properties of heat treated Inconel 718 superalloy by laser solid forming, Journal of Alloys and Compounds, 746 (2018) 159- 167. https://doi.org/10.1016/j.jallcom.2018.02.268

Q. Zhi, J. Niu, X. Tan, R. Pei, Y. Liu, Y. Chen, W. Liu, Effect of scanning process and heat treatment on microstructure and mechanical property of Inconel 718 fabricated by selective laser melting, Journal of Materials Engineering and Performance, 32 (21) (2023) 9515-9524. https://doi.org/10.1007/s11665-023-07828-2

W. Huang, J. Yang, H. Yang, G. Jing, Z. Wang, X. Zeng, Heat treatment of Inconel 718 produced by selective laser melting: Microstructure and mechanical properties, Materials Science and Engineering: A, 750 (2019) 98-107. https://doi.org/10.1016/j.msea.2019.02.046

N.Y.S. Tham, G.R.S. Tay, B. Yao, K. Wu, Z. Dong, Effect of aging parameters on Inconel 718 fabricated by laser directed energy deposition, Chinese Journal of Mechanical Engineering: Additive Manufacturing Frontiers, 2 (4) (2023) 100101. https://doi.org/10.1016/j.cjmeam.2023.100101

G.A. Rao, M. Kumar, M. Srinivas, D.S. Sarma, Effect of standard heat treatment on the microstructure and mechanical properties of hot isostatically pressed superalloy inconel 718, Materials Science and Engineering: A, 355 (1) (2003) 114-125. https://doi.org/10.1016/S0921-5093(03)00079-0

L. Huang, Y. Cao, J. Zhang, X. Gao, G. Li, Y. Wang, Effect of heat treatment on the microstructure evolution and mechanical behaviour of a selective laser melted Inconel 718 alloy, Journal of Alloys and Compounds, 865 (2021) 158613. https://doi.org/10.1016/j.jallcom.2021.158613

ASM Handbook Committee, ASM Handbook: Heat Treating, Vol. 4, ASM International, Materials Park, 1991, p. 1795.

C. Slama, M. Abdellaoui, Structural characterization of the aged Inconel 718, Journal of Alloys and Compounds, 306 (1) (2000) 277-284. https://doi.org/10.1016/S0925-8388(00)00789-1

J. Huang, Z. Huang, H. Du, J. Zhang, Effect of aging temperature on microstructure and tensile properties of Inconel 718 fabricated by selective laser melting, Transactions of the Indian Institute of Metals, 75 (6) (2022) 1403-1410. https://doi.org/10.1007/s12666-021-02487-0

Z. Guoqing, L. Junxin, Z. Xiaoyu, L. Jin, W. Anmin, Effect of heat treatment on the properties of CoCrMo alloy manufactured by selective laser melting, Journal of Materials Engineering and Performance, 27 (5) (2018) 2281-2287. https://doi.org/10.1007/s11665-018-3351-5

A.D.J. Saldívar García, A.M. Medrano, A.S. Rodríguez, Formation of hcp martensite during the isothermal aging of an fcc Co-27Cr-5Mo-0.05C orthopedic implant alloy, Metallurgical and Materials Transactions A, 30 (5) (1999) 1177-1184. https://doi.org/10.1007/s11661-999-0267-6

Y. Koizumi, S. Suzuki, K. Yamanaka, B.-S. Lee, K. Sato, Y. Li, S. Kurosu, H. Matsumoto, A. Chiba, Straininduced martensitic transformation near twin boundaries in a biomedical Co–Cr–Mo alloy with negative stacking fault energy, Acta Materialia, 61 (5) (2013) 1648-1661. https://doi.org/10.1016/j.actamat.2012.11.041

Y. Zhang, W. Lin, Z. Zhai, Y. Wu, R. Yang, Z. Zhang, Enhancing the mechanical property of laser powder bed fusion CoCrMo alloy by tailoring the microstructure and phase constituent, Materials Science and Engineering: A, 862 (2023) 144449. https://doi.org/10.1016/j.msea.2022.144449

X.P. Tan, P. Wang, Y. Kok, W.Q. Toh, Z. Sun, S.M.L. Nai, M. Descoins, D. Mangelinck, E. Liu, S.B. Tor, Carbide precipitation characteristics in additive manufacturing of Co-Cr-Mo alloy via selective electron beam melting, Scripta Materialia, 143 (2018) 117-121. https://doi.org/10.1016/j.scriptamat.2017.09.022

T. Kilner, R.M. Pilliar, G.C. Weatherly, C. Allibert, Phase identification and incipient melting in a cast Co- Cr surgical implant alloy, Journal of Biomedical Materials Research, 16 (1) (1982) 63-79. https://doi.org/10.1002/jbm.820160109

M. Caudillo, M. Herrera–Trejo, M.R. Castro, E. Ramírez, C.R. González, J.I. Juárez, On carbide dissolution in an as-cast ASTM F-75 alloy, Journal of Biomedical Materials Research, 59 (2) (2002) 378-385. https://doi.org/10.1002/jbm.10001

F.Z. Hassani, M. Ketabchi, S. Bruschi, A. Ghiotti, Effects of carbide precipitation on the microstructural and tribological properties of Co–Cr–Mo–C medical implants after thermal treatment, Journal of Materials Science, 51 (9) (2016) 4495-4508. https://doi.org/10.1007/s10853-016-9762-5

I. Milošev, H.H. Strehblow, The composition of the surface passive film formed on CoCrMo alloy in simulated physiological solution, Electrochimica Acta, 48 (19) (2003) 2767-2774. https://doi.org/10.1016/S0013-4686(03)00396-7

B. Patel, G. Favaro, F. Inam, M.J. Reece, A. Angadji, W. Bonfield, J. Huang, M. Edirisinghe, Cobalt-based orthopaedic alloys: Relationship between forming route, microstructure and tribological performance, Materials Science and Engineering: C, 32 (5) (2012) 1222-1229. https://doi.org/10.1016/j.msec.2012.03.012

J.H. Hollomon, Tensile deformation, Transactions of the Metallurgical Society of AIME, 162 (1945) 268- 290.

M. Zubair, S. Sandlöbes, M.A. Wollenweber, C.F. Kusche, W. Hildebrandt, C. Broeckmann, S. Korte- Kerzel, On the role of Laves phases on the mechanical properties of Mg-Al-Ca alloys, Materials Science and Engineering: A, 756 (2019) 272-283. https://doi.org/10.1016/j.msea.2019.04.048

M. Zubair, S. Sandlöbes-Haut, M.A. Wollenweber, K. Bugelnig, C.F. Kusche, G. Requena, S. Korte-Kerzel, Strain heterogeneity and micro-damage nucleation under tensile stresses in an Mg–5Al–3Ca alloy with an intermetallic skeleton, Materials Science and Engineering: A, 767 (2019) 138414. https://doi.org/10.1016/j.msea.2019.138414

D. Yan, C.C. Tasan, D. Raabe, High resolution in situ mapping of microstrain and microstructure evolution reveals damage resistance criteria in dual phase steels, Acta Materialia, 96 (2015) 399-409. https://doi.org/10.1016/j.actamat.2015.05.038

T.R. Bieler, M.A. Crimp, Y. Yang, L. Wang, P. Eisenlohr, D.E. Mason, W. Liu, G.E. Ice, Strain heterogeneity and damage nucleation at grain boundaries during monotonic deformation in commercial purity titanium, JOM, 61 (12) (2009) 45- 52. https://doi.org/10.1007/s11837-009-0180-x

A. Dutta, D. Ponge, S. Sandlöbes, D. Raabe, Strain partitioning and strain localization in medium manganese steels measured by in situ microscopic digital image correlation, Materialia, 5 (2019) 100252. https://doi.org/10.1016/j.mtla.2019.100252

G. Zhu, L. Wang, J. Wang, J. Wang, J.-S. Park, X. Zeng, Highly deformable Mg–Al–Ca alloy with Al2Ca precipitates, Acta Materialia, 200 (2020) 236-245. https://doi.org/10.1016/j.actamat.2020.09.006

Published
2026/07/02
How to Cite
Zubair, M., Nur, K., ul Haq, E., Ahmed, F., Javed, M. A., Khan, M. J., Naveed, M. M., ul Hassan, M. M., & Abdullah, A. (2026). A comparative study of mechanical behaviour of heat-treated 3D printed In-718 and ASTM F75 alloys across multiple length scales. Journal of Mining and Metallurgy, Section B: Metallurgy, 62(1), 53-67. Retrieved from https://aseestant.ceon.rs/index.php/jmm/article/view/62709
Section
Original Scientific Paper